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Beilstein J. Org. Chem. 2008, 4, No. 18, doi:10.3762/bjoc.4.18
Graphical Abstract
Scheme 1: Pd-catalyzed allylic substitution of the gem-difluorinated allylic carbonates 1 and 4.
Scheme 2: Synthesis of trans-trans dimer 8 and syn-syn dimer 9.
Figure 1: X-ray structure of trans-trans dimer 8.
Scheme 3: Reaction of trans-trans dimer 8 with 3-benzoylthymine sodium / PPh3.
Scheme 4: Reaction of trans-trans dimer 8 with PPh3 / AgSbF6.